(b) Determination of the residual methanol residue

(b) Determination of the residual methanol residues in a production sample of a drug.

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Suggest procedures by which the following analyses might be carried out and indicate how you might attempt to validate them:
(a) A stability indicating assay of glipizide tablets. Glipizide absorbs in the UV and is a base.
(b) Determination of the residual methanol residues in a production sample of a drug.
(c) A limit test for the morphine content of a sample of diacetylmorphine.